RT Journal Article T1 In Situ Synthesis of Al-Based MMCs Reinforced with AlN by Mechanical Alloying under NH3 Gas A1 Caballero, Eduardo S. A1 Gómez Cuevas, Francisco de Paula A1 Ternero Fernández, Fátima A1 Astacio, Raquel A1 Montes Martos, Juan Manuel A1 Cintas Físico, Jesús AB Aluminum matrix composites (AMCs) reinforced by aluminum nitride were preparedby mechanical alloying followed by a simple press and sintering method. Milling began undervacuum and after a period of between 1 and 4 h, NH3 gas flow (1 cm3/s) was incorporated untilthe total milling time of 5 h was reached. Results show that in addition to the strain hardeningtaking place during mechanical alloying, NH3 plays an additional role in powder hardening. Thereby,the properties of the sintered compacts are strongly influenced by the amount of N incorporated intothe powders during milling and the subsequent formation of AlN during the consolidation process.The obtained AMC reaches tensile strengths as high as 459 MPa and hardness much higher than thatof the as-received aluminum compact. PB MDPI SN 1996-1944 YR 2018 FD 2018 LK http://hdl.handle.net/10272/14792 UL http://hdl.handle.net/10272/14792 LA eng NO Caballero, E. S. Gómez Cuevas, Francisco Paula Ternero, Fátima Astacio, R. Montes Martos, Juan Manuel Cintas, J.: "In Situ Synthesis of Al-Based MMCs Reinforced with AlN by Mechanical Alloying under NH3 Gas". Materials. Vol. 11(5), 823; https://doi.org/10.3390/ma11050823 NO Financial support of the Ministerio de Economia y Competitividad (MINECO/FEDER, Spain) through the research project DPI2015-69550-C2-1-P is gratefully acknowledged. DS Repositorio Institucional de la Universidad de Huelva RD 30 may 2026